Certificate CCE-1:
Sample origin: Human serum
Date of sample receipt: 10/7/2010
Receipt condition: Frozen -80C
Sample Designations: 74 samples in SE04 set
Storage at Intelimmune: Frozen -80C
Assay Method: LC/MS-MRM
Assay Date: 10/11 - 10/13/10
Sample volume: 250 uL
Results Key:
Limit of Quantification
25-(OH) VD3 10pg/mL (0.025nM)
25-(OH) VD2 10pg/mL (0.024nM)
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Certificate CCE-2:
Sample origin: Human serum
Date of sample receipt: 10/19/2010
Receipt condition: Frozen -80C
Sample Designations: 49 samples in SE04 set
Storage at Intelimmune: Frozen -80C
Assay Method: LC/MS-MRM
Assay Date: 10/29 - 11/01/10
Sample volume: 300-500 uL
Results Key:
Limit of Quantification
25-(OH) VD3 10pg/mL (0.025nM)
25-(OH) VD2 10pg/mL (0.024nM)
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Certificate CCE-3:
Sample origin: Human serum
Date of sample receipt: 10/19/2010
Receipt condition: Frozen -80C
Sample Designations: 49 samples in SE04 set
Storage at Intelimmune: Frozen -80C
Assay Method: LC/MS-MRM
Assay Date: 11/16 - 11/22/10
Sample volume: 200-500 uL
Results Key:
Limit of Quantification
25-(OH) VD3 10pg/mL (0.025nM)
25-(OH) VD2 10pg/mL (0.024nM)
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Certificate CCE-4:
Sample origin: Human serum
Date of sample receipt: 10/19/2010
Receipt condition: Frozen -80C
Sample Designations: 60 samples in SE04 set
Storage at Intelimmune: Frozen -80C
Assay Method: LC/MS-MRM
Assay Date: 11/22 - 11/24/10
Sample volume: 250 uL
Results Key:
Limit of Quantification
25-(OH) VD3 10pg/mL (0.025nM)
25-(OH) VD2 10pg/mL (0.024nM)
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